To: Chuca Marsh who wrote (238 ) 10/6/1999 9:12:00 AM From: Chuca Marsh Read Replies (1) | Respond to of 402
ON EDIT :birchmountain.com Analytical Method Development In March, 1999, Birch Mountain initiated an in-house program to develop analytical methods to resolve inconsistencies between SEM/EMP imaging and precious metals analysis, and to address the problem of repeatability. By adjusting experimental conditions, by carefully recording experimental conditions, and by systematically varying key parameters, Birch Mountain is deliberately striving to identify and control the variables causing the erratic results. We are using Birch Mountain's laboratory, and facilities and analytical instrumentation available in the Department of Geology at the University of Calgary. Significant results from Birch Mountain's recent in-house work are given in Table 5. Atomic absorption measurements carried out by Birch Mountain at the University of Calgary utilized three point standard additions calibration and deuterium arc background correction. Table 5. Summary of Birch Mountain in-house analytical method development results, 1998 bulk sample BJ98-008. Digest Extraction Collector Analysis Type Au (g/t) Pt (g/t) Pd (g/t) Reductive Static None FA/ICP3 0.593 0.132 0.015 Caustic Bottle roll Adsorption FA/ICP 0.008 0.002 1.01 Acidic Bottle roll Adsorption FA/ICP 0.008 0.004 1.90 Caustic Bottle roll Adsorption FA/ICP 0.009 nd 0.558 Acidic Static Chiddey FA/ICP 0.0008 nd 0.427 Acidic Static None AA4 4 to 6 na na 3Fire assay - ICP; Loring Laboratories Ltd., Calgary, AB. 4Atomic absorption, University of Calgary, Calgary, AB. na — not analyzed; nd — not detected Although Birch Mountain's testing has shown important values of gold and palladium, we have not yet been able to reproduce "hits" despite careful attention to replicating the conditions and procedures of runs which yielded positive results. We can not yet explain this lack of repeatability. It is unlikely, however, that contamination is responsible because we obtain similar results using different methods and laboratories. Results for sample BJ98-008 are summarized in Table 6. Table 6. Summary of assay and leach results, 1998 bulk sample BJ98-008. PS- ChuckaOilsofSands- Minerals of NEED...scarce mnetal...psst- FUEL CELL USES, see my Rhombic WRITINGS...LOL. rhombic.com Really BIG, all the PGM needs for FC Cars! OIL SANDS is PRIMARY!